withacnistin/iochroma

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Parameters affecting microwave-assisted extraction of withanolides.

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Focused microwave-assisted extraction was applied to the extraction of three main withanolides from airdried leaves of Iochroma gesnerioides, namely, withaferin A, iochromolide and withacnistin. Six extraction variables, i.e. nature and volume of extracting solvent, sample moisture, extraction time,

Analysis of selected withanolides in plant extract by capillary electrochromatography and microemulsion electrokinetic chromatography.

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Microemulsion electrokinetic chromatography (MEEKC) coupled with a diode-array detector was developed for the simultaneous analysis of natural steroidal compounds, withanolides including withaferin A, withacnistin and iochromolide. Optimal resolution was obtained with a microemulsion consisting of

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