trimethylamine/kapsasrohi

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Determination of trimethylamine in spinach, cabbage, and lettuce at alkaline pH by headspace solid-phase microextraction.

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Trimethylamine (TMA) found in some leafy vegetables, such as spinach, cabbage, and lettuce, at alkaline pH was identified and quantified using headspace solid-phase microextraction and gas chromatography-mass spectrometry (HS-SPME and GC-MS). HS-SPME conditions were optimized at an adsorption

Stereospecific labeling of the glycerol moiety: synthesis of 1,2-dioleoyl-sn-[3-3H]glycero-3-phospho(1-rac-glycerol).

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1,2-Dioleoyl-sn-[3-3H]glycero-3-phospho(1-rac-glycerol) was synthesized from 1,2-dioleoyl-sn-glycerol using a new radiosynthetic procedure. 1,2-Dioleoyl-sn-glycerol was oxidized to the corresponding aldehyde using pyridinium dichromate and pyridine. The aldehyde was reduced to the radiolabeled

Characterization of the spoilage potential of pure and mixed cultures of bacterial species isolated from tropical yellowfin tuna (Thunnus albacares).

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OBJECTIVE The spoilage potential of 28 bacterial strains isolated from spoiled raw yellowfin tuna was evaluated. RESULTS Bacterial species were inoculated in irradiated tuna matrix. Chemical changes, bacterial growth and sensory quality were monitored during aerobic storage at 8°C. Pseudomonas spp.,

Detection of carbofuran and metabolites directly or as their heptafluorobutyryl derivatives using gas-liquid or high-pressure liquid chromatography with different detectors.

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The gas chromatography of the heptafluorobutyryl derivatives of carbofuran, 3-ketocarbofuran and 3-hydroxycarbofuran is examined with electrolytic conductivity detection (halogen mode). The reaction consists of heating the compounds with heptafluorobutyric anhydride in the presence of trimethylamine

Gas chromatographic analysis of heptafluorobutyryl derivatives of some carbamate insecticides.

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The gas chromatography (GC) of a number of carbamate insecticides as their heptafluorobutyryl derivatives has been studied. The reaction makes use of heptafluorobutyric anhydride with trimethylamine in benzene as a catalyst. Conversion of the insecticides to their products is complete in 15-20 min

Sensory characteristics of spoilage and volatile compounds associated with bacteria isolated from cooked and peeled tropical shrimps using SPME-GC-MS analysis.

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The spoilage potential of six bacterial species isolated from cooked and peeled tropical shrimps (Brochothrix thermosphacta, Serratia liquefaciens-like, Carnobacterium maltaromaticum, Carnobacterium divergens, Carnobacterium alterfunditum-like and Vagococcus penaei sp. nov.) was evaluated. The

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